Wet Granulation
Dense, dust-free, compact granules.
Homogeneously distributed components.
Ideal extrusion properties.
High-shear granulation for dust-free and compact granules from powder
Wet granulation (also wet blending) in the high-shear mixer is a classic process for building up granules from powder. This process is used when rapid agglomeration to form relatively compact granules is desired and the solid, pre-applied starting materials have low adhesive properties of their own. Powdered substances, such as vitamins, trace elements and other food supplements, can be adjusted to the desired dosage in suitable carriers and mixed homogeneously. But liquid active ingredients, such as enzymes, can also be incorporated and distributed in a matrix – for example starch or cellulose – by means of wet granulation. The wet granules are then dried to dust-free particles.
The agglomerates/granules produced in this way have a compact, extremely stable structure with a higher density than spray agglomerates from the fluid bed. They have good flowability and can be pressed.
Alternatively, the moist mass also serves as a starting mixture for further processing into pellets by means of low-pressure extrusion.
The dried granules or extrudates can be protected or functionalized (release control, color branding, taste/odor masking and others) against external influences (moisture, UV light, …) with a subsequent coating.
The process is also suitable for dedusting powders. Here, oils are mixed into the powders very quickly and homogeneously. Application examples for this can be found in products for hair cosmetics, among others.
For this process, Glatt offers high-shear granulators with different batch sizes for use in the bulk solids processing industry.
Product properties of agglomerates from highshear wet granulation at a glance:
Dust-free
Particles
Compact
Structure
High
Bulk Density
Good
Flow Behavior
Good
Dosability
Good
Dispersibility
Good
Solubility
Wide
Grain Size Spectrum
Ideal Properties
for Extrusion
A product container is charged with powder and this is moistened or sprayed with melt to build up cohesive forces. The liquid can be polar or apolar and should be able to dissolve the powder surface. If necessary, a binder is added to strengthen the cohesive force. The metered distribution of the granulating liquid via a spray nozzle, as well as the simultaneous, vigorous mechanical mixing of all input materials, ensures uniform distribution of all components in the granules.
Depending on the downstream sieve, a wide particle size range with agglomerate sizes between 0.1 mm and 10 mm is possible.
Product examples for wet granulation
Starch, wet granulation + coating
Graphite, wet granulation
Iron, food supplements, extrusion
CoQ10, extrusion
Hair color, extrusion
The process of highshear wet granulation in detail
A binder liquid is added to powdery particles in a closed container, which has mixing tools and a chopper. Dense granules are formed via resulting liquid and solid bridges.
Learn more about this process in the video on the right.
Stable, very dense and compact agglomerates from powder by means of highshear granulation
Further information on this topic and related topics can also be found in the following publications:
Published article: ‘Outsourcing – Trust in competent partners’ PDF, English
Published article: ‘Food, feed and pet nutrition:
a convergence of industries’ PDF, English
Glatt Technical Paper: ‘Gentle and safe processes – Drying and product design in the vacuum fluid bed’. PDF, German
Published article: ‘How to Tame Recalcitrant Ingredients with Technological Processes’ PDF, English
Published article: ‘Spray agglomerating plant-based milk alternatives for optimised product properties’ PDF, English